By Y. Mastai
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Extra info for Advances in Crystallization Processes
2005). Bernstein et al. , 2005) obtained the crystal structure of the γ phase and also discovered a previously unknown anhydrous δ phase. Fig. 4. MNPU (right) and biphenyl thiol molecules used in the biphenyl thiol SAMs (1-7) – (left). , 2005) Initially, Hiremath et al. obtained the pure polymorph phases by varying solvents and temperature. The α-MNPU was obtained from crystallization in ethanol at 60°C, β-MNPU was obtained from crystallization in ethyl acetate at room temperature. The γ form was obtained by re-crystallization of the α or β forms in 95% ethanol.
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2005) Fig. 5. L-AAPP (Dressler and Mastai, 2007) Substrates for SAM preparation were prepared by vacuum deposition of thin gold films onto glass slides. The gold substrates were then immersed in 2mM L-AAPP ethanolic solutions overnight in order to receive the L-AAPP SAMs. L-AAPP was chosen as the molecule for self assembly since L-phenylalanine has already been shown to promote the stabilization of the α-form of L-glutamic acid in solution. In order to examine the effect of the SAMs on L-glutamic acid crystallization, a series of crystallization experiments were performed on the surfaces and in solutions.
Advances in Crystallization Processes by Y. Mastai