New PDF release: Advances in Crystallization Processes

By Y. Mastai

ISBN-10: 9535105817

ISBN-13: 9789535105817

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2005). Bernstein et al. , 2005) obtained the crystal structure of the γ phase and also discovered a previously unknown anhydrous δ phase. Fig. 4. MNPU (right) and biphenyl thiol molecules used in the biphenyl thiol SAMs (1-7) – (left). , 2005) Initially, Hiremath et al. obtained the pure polymorph phases by varying solvents and temperature. The α-MNPU was obtained from crystallization in ethanol at 60°C, β-MNPU was obtained from crystallization in ethyl acetate at room temperature. The γ form was obtained by re-crystallization of the α or β forms in 95% ethanol.

Z. Physik. Chem. 1899, 28, 494. Tetrahedron: Asym. , 2008, 4, 519 [4] Scheldon, R. A. Chirotechnology, Marcel Dekker Inc. Y 1993 [5] Novák, T; Schindler, J; Ujj, V; Czugler, M; Fogassy, E; Keglevich, Gy: Tetrahedron: Asymmy. 2006, 2599. [6] Ujj V; Schindler J; Novák T; Czugler M; Fogassy E; Keglevich Gy: Tetrahedron: Asymm. : Chem. , 2007, 3990-3996. : Chem. , 2007, 1071-1073. S. I. , 2007, 37, 55-60. : Organic & Biomolecular Chemistry 2010, 8, 347-359. ; Hirayama, N. ; Grofcsik, A. J. Chem. ; Reck, G.

2005) Fig. 5. L-AAPP (Dressler and Mastai, 2007) Substrates for SAM preparation were prepared by vacuum deposition of thin gold films onto glass slides. The gold substrates were then immersed in 2mM L-AAPP ethanolic solutions overnight in order to receive the L-AAPP SAMs. L-AAPP was chosen as the molecule for self assembly since L-phenylalanine has already been shown to promote the stabilization of the α-form of L-glutamic acid in solution. In order to examine the effect of the SAMs on L-glutamic acid crystallization, a series of crystallization experiments were performed on the surfaces and in solutions.

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Advances in Crystallization Processes by Y. Mastai


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